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- W2024760129 abstract "The separation of vitamin D3 metabolites and their analogues by high-pressure liquid chromatography was investigated using a Zorbax SIL column. Each metabolite can be separated effectively with a solvent consisting of 2% methanol-methylene chloride or gradient elution from 0.02% to 6% methanol-methylene chloride. The C-24 epimers of 1α,24-dihydroxy- and 1α,24,25-trihydroxy-vitamin D3 are resolved as their free forms, while the epimers of 24-hydroxy- and 24,25-dihydroxy-vitamin D3 can be separated as their trimethylsilyl derivatives." @default.
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- W2024760129 date "1976-04-01" @default.
- W2024760129 modified "2023-10-14" @default.
- W2024760129 title "Separation of vitamin D3 metabolites and their analogues by high-pressure liquid chromatography" @default.
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- W2024760129 doi "https://doi.org/10.1016/s0021-9673(00)86786-2" @default.
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