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- W2024765211 abstract "Abstract Six chiral di-N-p-toluenesulphonyl diazacoronands derived from L-tartaric acid were synthesized by the modified Richman Atkins procedure. The deprotection of isopropylidene acetal led to the formation of compounds 7 possessing an 1,2-diol subunit. 1H and 13C NMR, UV and MS techniques were used for structure assignment. The determination of the X-ray structure of compounds 6a and 7b pointed to a variety of ring conformations. The shape of the molecules is to a great extent determined by a system of intra- and intermolecular hydrogen bonds of a O…O and C…O nature. Compound 7b was found to form a supramolecular assembly (H-bonded dimers) both in solution and in solid state. Complexation studies of this group of compounds suggest that this process is mediated by the hydroxyl and sulfonyl group oxygen atoms." @default.
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- W2024765211 date "1995-06-01" @default.
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- W2024765211 title "Synthesis and structure of chiral diazacoronands derived from L-tartaric acid1" @default.
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- W2024765211 doi "https://doi.org/10.1080/10610279508029482" @default.
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