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• W2024779989 abstract "Treatment of cyclopropyl ketones with TiCl4-n-Bu4NI mixed reagent provides (Z)-titanium enolates which afford syn-α-iodethyl-β-hydroxyketones stereoselectively upon subsequent reaction with various aldehydes. The aldol adducts are cyclized into trans-acyltetrahydrofurans in good yield by active alumina. In contrast, the use of Et2AlI in place of TiCl4-n-Bu4NI provides the corresponding anti aldol adducts with high stereoselectivity. These methods can complementarily provide both syn and anti isomers of α-iodoethyl-β-hydroxyketones from cyclopropyl ketones and aldehydes." @default.
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• W2024779989 date "2001-02-01" @default.
• W2024779989 modified "2023-10-18" @default.
• W2024779989 title "Enolate formation from cyclopropyl ketones via iodide-induced ring opening and its use for stereoselective aldol reaction" @default.
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• W2024779989 doi "https://doi.org/10.1016/s0040-4020(00)01094-2" @default.
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