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• W2024891154 abstract "Monolithic molybdenum oxide aerogels and xerogels were synthesized by sol–gel methods using a variety of sol compositions from the system Mo(OC3H7)5/MoCl3(OC3H7)2/acetonitrile/nitric acid/H2O. The aerogels were found to be of density 0.1–0.2 g/cm3 with surface areas between 150–180 m2/g. The xerogels had densities between 1.5–2.0 g/cm3 and surface areas less than 10 m2/g. The as-prepared gels are amorphous materials with compositions corresponding to MoO3−x·1.0H2O·0.3CH3NH2. Crystallization to the orthorhombic phase occurs at 350°C. Electrochemical measurements demonstrate that lithium can be intercalated reversibly into the aerogel structure. An ambient pressure drying method based on the use of low surface tension solvents produced monolithic gels with high surface areas (250–270 m2/g) and densities between 0.7–0.9 g/cm3." @default.
• W2024891154 created "2016-06-24" @default.
• W2024891154 creator A5062699080 @default.
• W2024891154 creator A5064544688 @default.
• W2024891154 date "1998-04-01" @default.
• W2024891154 modified "2023-10-17" @default.
• W2024891154 title "Sol–gel synthesis and characterization of molybdenum oxide gels" @default.
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• W2024891154 doi "https://doi.org/10.1016/s0022-3093(98)00018-0" @default.
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