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- W2024910208 abstract "The rational selection of an optimal gradient in reversed-phase liquid chromatography is discussed from two viewpoints. Firstly, a general expression is derived for the numerical calculation of retention data for the case when the relationship between the capacity factor, k , and the mobile phase composition, φ, is known. For a linear gradient a graphical solution is demonstrated and analytical solutions are presented for simple but widely applicable k φ relationships. Retention data thus calculated agree well with experimental results. Secondly, the multi-component solubility parameter theory is used to predict the k φ relationship. Modification of the stationary chemically bonded phase under the influence of the organic modifier is introduced to improve the accuracy of the predictions. Empirical correlations using solubility parameters are presented as an alternative to the theoretical expressions." @default.
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- W2024910208 date "1978-02-01" @default.
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- W2024910208 title "Gradient selection in reversed-phase liquid chromatography" @default.
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- W2024910208 doi "https://doi.org/10.1016/s0021-9673(00)81008-0" @default.
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