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- W2024918879 abstract "Abstract Single crystals of L -histidine dihydrochloride were obtained from an aqueous solution containing L -histidine and diluted hydrochloric acid. The crystals are monoclinic with the cell dimensions, a = 5.243(2) Å, b = 7.257(1) Å, c = 13.350(1) Å, β = 92.65(1)°, space group P 2 1 , and Z = 2. Least-squares refinement using 2685 X-ray (MoK α ) reflections has led to an R factor of 0.029. The L -histidine moiety in this complex exists as a dication where the carboxylic group as well as the amino nitrogen and the imidazole ring are protonated. Based on the N–C α –C β –C γ torsion angle ( ψ ⊥ = 57.1°), the conformation of the histidine molecule in this structure is g + , whereas the conformation in the orthorhombic form of this complex (reported earlier) is g − . There are no direct contacts (hydrogen bonds) between the histidine moieties as all the intermolecular bonding seem to involve Cl − ions." @default.
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- W2024918879 date "1995-02-01" @default.
- W2024918879 modified "2023-09-23" @default.
- W2024918879 title "Crystal and molecular structure of <i>L</i>-(<i>S</i>)-histidine dihydrochloride (monoclinic form)" @default.
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