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- W2024954014 abstract "We report the development of a multicatalytic, one-pot, asymmetric Michael/Stetter reaction between salicylaldehydes and electron-deficient alkynes. The cascade proceeds via amine-mediated Michael addition followed by an N-heterocyclic carbene-promoted intramolecular Stetter reaction. A variety of salicylaldehydes, doubly activated alkynes, and terminal, electrophilic allenes participate in a one-step or two-step protocol to give a variety of benzofuranone products in moderate to good yields and good to excellent enantioselectivities. The origin of enantioselectivity in the reaction is also explored; E/Z geometry of the reaction intermediate as well as the presence of catalytic amounts of catechol additive are found to influence reaction enantioselectivity." @default.
- W2024954014 created "2016-06-24" @default.
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- W2024954014 date "2010-07-16" @default.
- W2024954014 modified "2023-10-12" @default.
- W2024954014 title "Multicatalytic, asymmetric Michael/Stetter reaction of salicylaldehydes and activated alkynes" @default.
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- W2024954014 doi "https://doi.org/10.1073/pnas.1002830107" @default.
- W2024954014 hasPubMedCentralId "https://www.ncbi.nlm.nih.gov/pmc/articles/2996425" @default.
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