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- W2024963995 abstract "The molecular structure of the cycloadduct from 4-bromo-N-methoxycarbonylazepine and tetracyanoethylene has been shown to be 6-bromo-8,8,9,9-tetracyano-2-methoxycarbonyl-2-azabicyclo[3,2,2]nona-3,6-diene by the results of a single-crystal X-ray investigation. The crystals are monoclinic, a= 19·25 ± 0·03, b= 10·87 ± 0·02, c= 8·98 ± 0·02 Å, β= 101° 30′± 15′. The space group is P21/a with four molecules of C14H8BrN5O2,½C7H8 in the unit cell. Refinement of the structure produced some anomalous results, and a critical examination of these difficulties led to the detection of a cocrystallised isomer in approximately 15% of the total number of molecular sites. This isomer apparently originated from a cycloaddition involving 3-bromo-N-methoxycarbonylazepine and tetracyanoethylene. The molecular geometry of the ring system of the major isomer is described." @default.
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- W2024963995 date "1967-01-01" @default.
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- W2024963995 title "Crystal and molecular structure of the cycloadducts formed by mono-bromo-N-methoxycarbonylazepine and tetracyanoethylene" @default.
- W2024963995 doi "https://doi.org/10.1039/j29670000112" @default.
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