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• W2024987058 startingPage "13712" @default.
• W2024987058 abstract "We report a template-free strategy based on steric repulsion for the isolation of discrete columnar aggregates of macrocycles. Specifically, introduction of sterically-demanding trityl-derived substituents at the periphery of Pt(4) Schiff base macrocycles limits the otherwise infinite one-dimensional columnar aggregation to discrete tetrameric and hexameric assemblies. Single crystal X-ray diffraction studies of these compounds reveal discrete nanotubes of finite length that pack inefficiently resulting in three-dimensional networks of interconnected void space. The discrete assemblies were studied by N(2) adsorption and show enhanced surface area when stacked. In the absence of bulky substituents the macrocycles are nonporous. This strategy for engineering discrete supramolecular macrocyclic aggregates may be generalized to other columnar assembling systems." @default.
• W2024987058 created "2016-06-24" @default.
• W2024987058 creator A5030607010 @default.
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• W2024987058 creator A5081446249 @default.
• W2024987058 creator A5084063590 @default.
• W2024987058 date "2012-09-20" @default.
• W2024987058 modified "2023-09-26" @default.
• W2024987058 title "Sterically-Limited Self-Assembly of Pt₄Macrocycles into Discrete Non-covalent Nanotubes: Porous Supramolecular Tetramers and Hexamers" @default.
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• W2024987058 doi "https://doi.org/10.1002/chem.201201536" @default.
• W2024987058 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/22997016" @default.
• W2024987058 hasPublicationYear "2012" @default.

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