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- W2024998216 abstract "Abstract At low monomer concentrations the use of TMEDA and THF as promoters in the n-BuLi-initiated polymerization of butadiene results in the formation of vinyl cyclopentane chain units in addition to the normal 1,4- and 1,2-microstructure. TMEDA is more effective than THF in promoting formation of the cyclic structure and with TMEDA the cyclic content of the polybutadiene can be as high as 45 wt %. Surprisingly, the use of high levels of THF in conjunction with n-BuLi and TMEDA can actually suppress the formation of cyclic units. The sodium counterion is also shown to yield the cyclic structure with the same promoters." @default.
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- W2024998216 date "1981-03-01" @default.
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- W2024998216 title "Observations on the preparation of polybutadiene containing vinyl cyclopentane units" @default.
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- W2024998216 doi "https://doi.org/10.1016/0032-3861(81)90051-3" @default.
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