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- W2025101743 abstract "A new, convenient and stereoselective route to the synthesis of (25R)-cholest-5-ene-3β,26-diol (1) and its radiolabeled analog 4 is described. The key step is a Julia condensation of sulfone 6 with aldehyde 12 to furnish compound 13. Further reduction of the α-hydroxysulfone moiety afforded 22,23-unsaturated i-steroid 14. The double was reduced by hydrogen and by tritium to provide substrates for the preparation of 1 and 4, respectively." @default.
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- W2025101743 date "1997-06-01" @default.
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- W2025101743 title "Synthesis of (25R)-cholest-5-ene-3β, 26-diol and its radiolabeled analog" @default.
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- W2025101743 doi "https://doi.org/10.1016/s0040-4039(97)00750-8" @default.
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