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- W2025129239 abstract "Abstract Pd-Ag electroplated films, codeposited from a glycine-glycinate containing electrolyte at pH 9.5, were studied by X-ray diffraction. The crystallographic structure of the films was markedly influenced by the potential applied during the plating and by adding sodium benzaldehyde-2,4-disulphonate (BDS) to the electrolyte. In the absence of BDS, at +100 mV with respect to a reversible hydrogen electrode (RHE) a two-phase deposit was generated consisting of almost pure palladium and silver. At more negative potentials, more or less homogeneous alloys were obtained, exhibiting a deformed and partly contracted lattice. In the presence of BDS and at -50 mV (RHE), no deformation was observed but, as an extraordinary result, a linear lattice contraction of about 0.4%. Owing to the hydrogen codeposition and insertion, the lattice was dilated, overcompensating the contraction. In all cases, an anisotropy effect, compared with metallurgically prepared alloys, was observed which was influenced by the nature of the substrate and by the electrolyte composition. Additional hydrogen-charging and hydrogen-discharging experiments revealed distinct correlation between the homogeneity of the alloy and the hydrogen diffusibility in the alloy." @default.
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- W2025129239 date "1993-09-01" @default.
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- W2025129239 title "Morphological effects on electrodeposited Pd-Ag films due to the electroplating conditions" @default.
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