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- W2025318204 abstract "2,4,4,6-Tetraaryl-4 H -thiopyrans Ia - Ig react smoothly with carbon disulfide solution of chlorine already at 0 °C yielding the corresponding 3,5-dichloro derivatives IIa - IIg . With longer reaction time and temperature raised to 20 °C, the 4 H -thiopyrans Ia - Ie gave exclusively the trichloro derivatives IIIa - IIIe whereas If and Ig underwent a nonselective chlorination leading to multicomponent mixtures of products. Isolation of sulfoxides IVa and IVe from the chlorination of Ia and Ie (upon hydrolysis of the reaction mixture) allowed us to formulate the reaction mechanism for the formation of compounds type III . 1 H, 13 C NMR, and mass spectra of the prepared compounds are discussed in detail." @default.
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- W2025318204 date "2010-08-18" @default.
- W2025318204 modified "2023-10-02" @default.
- W2025318204 title "ChemInform Abstract: Reactions of 2,4,4,6-Tetraaryl-4H-thiopyrans with Chlorine: An Unusual Reaction Route." @default.
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- W2025318204 doi "https://doi.org/10.1002/chin.199517059" @default.
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