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- W2025381114 abstract "The reaction of aromatic and aliphatic aldehydes with hypophosphorus acid under microwave irradiation was examined. The reaction gave a mixture of a racemic pair of bis(α-hydroxyalkyl)phosphinic acids and acetal derivatives from the corresponding bis(α-hydroxyalkyl)phosphinic acids of meso-stereochemistry in good yield. The difference in solubility in organic solvents due to polarity allowed us to readily separate these compounds. This method constitutes an easy, rapid, and good-yielding preparation and separation of bis(α-hydroxyalkyl) phosphinic acid diastereoisomers from simple starting materials using microwave irradiation." @default.
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- W2025381114 date "2006-07-18" @default.
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- W2025381114 title "A Novel Method for the Separation of Bis(α-hydroxyalkyl)phosphinic Acid Diastereoisomers via Formation of Novel Cyclic Phosphinic Acids" @default.
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- W2025381114 doi "https://doi.org/10.1021/jo060547h" @default.
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