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• W2025506067 abstract "We present a robust data analysis method of time-resolved x-ray absorption spectroscopy experiments suitable for chemical speciation and structure determination of reaction intermediates. Chemical speciation is done by principal component analysis (PCA) of the time-resolved x-ray absorption near-edge structure data. Structural analysis of intermediate phases is done by theoretical modeling of their extended x-ray absorption fine-structure data isolated by PCA. The method is demonstrated using reduction and reoxidation of Cu-doped ceria catalysts where we detected reaction intermediates and measured fine details of the reaction kinetics. This approach can be directly adapted to many time-resolved x-ray spectroscopy experiments where new rapid throughput data collection and analysis methods are needed." @default.
• W2025506067 created "2016-06-24" @default.
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• W2025506067 date "2008-12-15" @default.
• W2025506067 modified "2023-09-27" @default.
• W2025506067 title "Solving the structure of reaction intermediates by time-resolved synchrotron x-ray absorption spectroscopy" @default.
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• W2025506067 doi "https://doi.org/10.1063/1.3040271" @default.
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