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- W2025602023 abstract "Abstract Two mixed ligand complexes of copper(II) azide with 3-picoline and 4-picoline, namely di-μ(1,1)-azido-μ( O , O )-nitrato)( O -nitrato)tetrakis(3-picoline)dicopper(II) ( 1 ) and catena-di-μl(1,3)-azido-[di-μ(1,1)-azido-bis(4-picoline)dicopper(II)] ( 2 ), have been synthesized and characterized by X-ray crytallography. The structure of complex 1 consists of asymmetric dimeric units in which Cu(1) is six-coordinated to two nitrogen atoms from the picoline molecules, two nitrogen atoms of the two μ(1,1) bridging azido ligands and two oxygen atoms of the two nitrate anions. Cu(2) is also six-coordinated to two nitrogen atoms of the other two picolines, two nitrogen atoms of the two μ(1,1) bridging azido ligands, an oxygen atom of the aqua molecule and an oxygen atom of the μ( O , O ) bridging nitrato group. The structure of complex 2 features distorted square pyramidal Cu II coordination geometry, centrosymmetric di-μ(1,1) azido bridged Cu 2 N 2 rings and di-μ(1,3) azido bridges which link the binuclear Cu 2 (4-picoline) 2 (N 3 ) 2 moieties into chains along the short α-axis. The IR and electronic spectra of the solid complexes are presented and discussed." @default.
- W2025602023 created "2016-06-24" @default.
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- W2025602023 date "1993-12-01" @default.
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- W2025602023 title "Synthesis, spectroscopic and crystal structure study of di-μ)1,1)-azido-μ(O,O)-nitrato(O-nitrato)tetrakis(3-picoline)aquadicopper(II) and catena-di-μ(1,3)-azido-[di-μ(1,1)-azido-bis(4-picoline)dicopper(II)] [Cu2(N3)2(NO3)2(3-picoline)4(H2O)] and Cu(4-picoline)(N3)2" @default.
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- W2025602023 doi "https://doi.org/10.1016/s0277-5387(00)80065-0" @default.
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