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• W2025688889 abstract "In Part 1, the promising hydrogen storage properties of the combined systems of Li3AlH6/LiBH4 and Al/LiBH4, exhibiting the favorable formation of AlB2 during dehydrogenation, were presented based on TGA and XRD analyses. The present Part 2 describes the characterization of the intermediate and final products of the dehydrogenation and rehydrogenation of the above systems by multinuclear solid-state NMR characterization. This work has also verified that the presence of Al resulted in the re-formation of LiBH4 occurring at a much lower temperature and H2 pressure, under which conditions the dehydrogenation product from LiBH4 alone does not show any degree of rehydrogenation. NMR studies mainly identified various reaction intermediates for LiBH4 dehydrogenation/rehydrogenation reactions. Unlike the XRD studies, the AlB2 formation, in particular, could not be unambiguously confirmed by NMR. 27Al NMR showed that aluminum was mainly involved in various Li—Al alloy formations. The catalytic role of Al in the LiBH4 hydrogen storage reactivity could be achieved by a reversible cycle of the Al + LiH ↔ LiAl + 1/2H2 reaction." @default.
• W2025688889 created "2016-06-24" @default.
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• W2025688889 date "2011-03-10" @default.
• W2025688889 modified "2023-10-18" @default.
• W2025688889 title "Reaction Mechanisms in the Li₃AlH₆/LiBH₄ and Al/LiBH₄ Systems for Reversible Hydrogen Storage. Part 2: Solid-State NMR Studies" @default.
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• W2025688889 doi "https://doi.org/10.1021/jp109113f" @default.
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