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- W2025821782 endingPage "3784" @default.
- W2025821782 startingPage "3775" @default.
- W2025821782 abstract "Two different copolymers, i.e., poly(tert-BuA-co-chloromethylstyrene) and poly(tert-BuA-co-HEA), were synthesized by reversible addition−fragmentation (RAFT) polymerization. A poly(tert-BuA-co-chloromethylstyrene) copolymer was subsequently modified by thioglucose using a thio−halogen click nucleophilic substitution reaction. A poly(tert-BuA-co-HEA) copolymer was subsequently modified by p-toluenesulfonyl chloride, followed by sugar functionalization (galactose) via a nucleophilic substitution reaction. The resultant glycopolymers were characterized by NMR, FTIR, and GPC analyses. Both glyco-modification procedures were shown to be highly efficient with yields close to 100%. After deprotection of the tert-butyl groups to form carboxylic acid functionality, the copolymers were assembled onto positively charged gold nanoparticle (GNPs) surfaces using a layer-by-layer (LbL) methodology to yield sugar-functional GNPs. The glycopolymer-coated nanoparticles were characterized by transmission electron microscopy (TEM), UV−vis spectroscopy, dynamic light scattering (DLS), zeta-potential, and X-ray photoelectron spectroscopy (XPS). Finally, the presence of accessible sugar moieties on the surface of the GNPs was confirmed by a binding assay with Con A." @default.
- W2025821782 created "2016-06-24" @default.
- W2025821782 creator A5001395511 @default.
- W2025821782 creator A5003954971 @default.
- W2025821782 creator A5016059121 @default.
- W2025821782 creator A5017902199 @default.
- W2025821782 creator A5045756182 @default.
- W2025821782 creator A5080804325 @default.
- W2025821782 date "2010-03-10" @default.
- W2025821782 modified "2023-10-14" @default.
- W2025821782 title "Glycopolymer Decoration of Gold Nanoparticles Using a LbL Approach" @default.
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