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• W2025970018 abstract "The stepwise formation of the bifunctional σ3,λ4-phosphanediyl complex (2,4,6-But3C6H2O)(Cl)PMoCp(CO)2 (4) (R = 2,4,6-But3C6H2O) is reported. The primary metallo-chlorophosphine (R)(Cl)PMoCp(CO)3 (3) is isolated in almost quantitative yield from the reaction of RPCl2 (1) with Na[MoCp(CO)3] (2). Decarbonylation of 3 affords 4. The reactivity of 4 towards different nucleophiles is discussed. The identities of all new compounds are documented by analytical as well as spectroscopic (IR, MS, 1H, 13C and 31P NMR) data; the X-ray structure of (R)(Cl)PMoCp(CO)3 (3) is reported." @default.
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• W2025970018 date "1993-05-01" @default.
• W2025970018 modified "2023-10-03" @default.
• W2025970018 title "Stepwise synthesis and reactivity of a chlorine-functionalized δ3,λ4-phosphanediyl complex; X-ray crystal structure of (2,4,6-But3C6H2O)(Cl)PMoCp(CO)3" @default.
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• W2025970018 doi "https://doi.org/10.1016/s0277-5387(00)88221-2" @default.
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