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• W2026042792 abstract "This work examines the robustness of fitting of parameters describing conformational exchange (kex, pa/b, and Δω) processes from CPMG relaxation dispersion data. We have analyzed the equations describing conformational exchange processes for the intrinsic inter-dependence of their parameters that leads to the existence of multiple equivalent solutions, which equally satisfy the experimental data. We have used Monte-Carlo simulations and fitting to the synthetic data sets as well as the direct 3-D mapping of the parameter space of kex, pa/b, and Δω to quantitatively assess the degree of the parameter inter-dependence. The demonstrated high correlation between parameters can preclude accurate dynamics parameter estimation from NMR spin-relaxation data obtained at a single static magnetic field. The strong parameter inter-dependence can readily be overcome through acquisition of spin-relaxation data at more than one static magnetic field thereby allowing accurate assessment of conformational exchange properties." @default.
• W2026042792 created "2016-06-24" @default.
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• W2026042792 date "2006-05-01" @default.
• W2026042792 modified "2023-10-09" @default.
• W2026042792 title "Faithful estimation of dynamics parameters from CPMG relaxation dispersion measurements" @default.
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• W2026042792 doi "https://doi.org/10.1016/j.jmr.2006.01.010" @default.
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