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- W2026044034 abstract "Abstract A novel Ru(II)(COD) dimer containing triply-bridging chloride ligands has been prepared and its crystal structure determined. The metal atoms each contain axial COD ligands and are separated by a distance of 3.251 A. Both transition metals possess octahedral coordination geometries. One contains a coordinated molecule of acetonitrile and the other contains an axial halide ligand. Electrochemical investigations show that the complex undergoes two one-electron oxidations that satisfy the criteria for a fully reversible diffusion controlled process. An improved method of preparing this dimeric Ru(II) cycloolefin complex is also presented. The crystals are monoclinic, space group C2/c, a=21.258(6), b=7.179(2), c=27.068(7) A, β=93.18(2)°, V=4124(2) A3. Convergence to conventional R values of R=0.0368 and Rw=0.0394 with a goodness-of-fit of 0.95 was obtained for 226 variable parameters and 2710 reflections with I>0σ(I)." @default.
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- W2026044034 date "1994-10-01" @default.
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- W2026044034 title "Electrochemical behavior and X-ray crystal structure of the unusual dimeric ruthenium(cyclooctadiene) complex, (tri-μ-chloro)(chloro)(acetonitrile)bis(η4-cyclooctadiene)-diruthenium(II)" @default.
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- W2026044034 doi "https://doi.org/10.1016/0020-1693(94)04119-9" @default.
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