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- W2026063507 abstract "The first total synthesis of the cytotoxic marine macrolide enigmazole A has been completed in 22 steps (longest linear sequence). The sensitive, densely functionalized 2,4-disubstituted oxazole fragment was constructed using an efficient Negishi-type coupling of an oxazol-2-ylzinc reagent formed directly from the parent ethyl 2-iodooxazole-4-carboxylate by zinc insertion. Other key steps include a hetero-Diels−Alder cycloaddition to form the central embedded pyran ring, a Wittig reaction to unite Eastern and Western hemispheres, and a ring size-selective Keck macrolactonization." @default.
- W2026063507 created "2016-06-24" @default.
- W2026063507 creator A5037671886 @default.
- W2026063507 creator A5056958049 @default.
- W2026063507 creator A5067818150 @default.
- W2026063507 date "2010-06-30" @default.
- W2026063507 modified "2023-10-18" @default.
- W2026063507 title "Total Synthesis of Enigmazole A from <i>Cinachyrella enigmatica</i>. Bidirectional Bond Constructions with an Ambident 2,4-Disubstituted Oxazole Synthon" @default.
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- W2026063507 doi "https://doi.org/10.1021/ja1016975" @default.
- W2026063507 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/20590095" @default.
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