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- W2026132508 abstract "A comparative study has been performed on the selective reduction of cyclotron-produced [11C]carbon dioxide to [11C]formaldehyde with solutions of various complex metal hydrides at temperatures between −52 and +25°C. Under optimal reaction conditions, lithium tetrahydridoaluminate gave the highest yield of [11C]formaldehyde (58%, decay-corrected), followed by lithium triethylhydridoborate (34%) and sodium tetrahydridoborate (22%). Radiochemically pure [11C]formaldehyde could be obtained with lithium tetrahydridoaluminate and sodium tetrahydridoborate, but not with lithium triethyl hydridoborate. The produced [11C]formaldehyde was used for the synthesis of [1-11C]1,2,3,4-tetrahydro-β-carboline derivatives by the Pictet–Spengler reaction." @default.
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- W2026132508 date "1998-12-01" @default.
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- W2026132508 title "Low temperature synthesis of no-carrier-added [11C]formaldehyde with metal hydrides and preparation of [1-11C]1,2,3,4-Tetrahydro-β-Carboline Derivatives" @default.
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- W2026132508 doi "https://doi.org/10.1016/s0969-8043(97)10156-7" @default.
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