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- W2026324638 abstract "In this paper we describe the preparation of a hexapeptide library by combinatorial synthesis and the identification of a peptide with sequence Ser-Asn-Leu-His-Pro-Lys, which showed good affinity (Keq = 3.4 × 104 M−1) towards the mycotoxin ochratoxin A (OTA). An immunoaffinity-like stationary phase supporting such a hexapeptide was used to develop a solid-phase extraction method for the quantification of OTA in wine samples at concentration levels down to 0.10 μg l−1. Several different wine samples fortified with OTA at 2 and 4 μg l−1 levels showed recovery of 94.7% and 98.4% at 2.0 and 4.0 μg l−1, respectively, without any effect on the extraction efficiency of the matrix. The efficacy of this approach was successfully tested by comparison with an immunoaffinity extraction performed on commercial cartridges." @default.
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- W2026324638 date "2007-12-01" @default.
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- W2026324638 title "Solid-phase extraction of ochratoxin A from wine based on a binding hexapeptide prepared by combinatorial synthesis" @default.
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- W2026324638 doi "https://doi.org/10.1016/j.chroma.2007.10.057" @default.
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