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- W2026462876 abstract "A new, mild, general, and efficient synthesis of N-protected α-amino acid hydrazides is described. This two-step preparation uses N-aminophthalimide as protected hydrazine to prepare N-protected α-amino acid hydrazide precursors, and subsequent dephthaloylation with an aminomethyl polystyrene resin yields N-protected α-amino acid hydrazides. It has the advantages of avoiding the use of the toxic hydrazine reagent and being compatible with the most commonly used N-protecting groups. This strategy is particularly interesting in the case of N-(9-fluorenylmethoxycarbonyl)-protected amino acids. Within the limits of chiral HPLC detection, no epimerization is apparent." @default.
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- W2026462876 date "2009-03-16" @default.
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- W2026462876 title "Enantioselective Synthesis of N-Protected α-Amino Acid Hydrazides" @default.
- W2026462876 doi "https://doi.org/10.1055/s-0028-1088013" @default.
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