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- W2026529713 abstract "The enantioselective total synthesis of the dual-specificity phosphatase inhibitor (−)-bitungolide F has been achieved using two convergent routes. Both strategies feature an asymmetric boron-mediated pentenylation, a stereoselective aldol, and a hydroxyl-directed 1,3-anti-reduction in order to control the stereogenic centers at C4, C5, C9, and C11. Whereas the first total synthesis was achieved in 11 steps and 14.6% overall yield using an Evans-type asymmetric alkylation, the second was completed in 9 steps and 11.4% overall yield using a highly enantioselective organocatalytic Michael addition as a key step and a protecting group free strategy." @default.
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- W2026529713 date "2010-08-20" @default.
- W2026529713 modified "2023-10-09" @default.
- W2026529713 title "Two Concise Total Syntheses of (−)-Bitungolide F" @default.
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- W2026529713 doi "https://doi.org/10.1021/ol101659y" @default.
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