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- W2026677369 abstract "Reactions of tetrasulfur tetranitride (S 4 N 4 ) with aryl and alkyl bromomethyl ketones 1 in chlorobenzene at reflux temperature gave 3,5-diaroyl- and 3,5-diacyl-1,2,4-thiadiazoles 2 in 17-60% yields. No 1,2,5-thiadiazoles were detected. By heating of the two reactants at 115° without the solvent were also obtained 2 in 5-13% yields. Hydrolysis of 2 with sodium hydroxide in a mixture of ethanol, ethyl acetate, and water (v:v, 4:2:1) at 75 o to 85 o afforded the heretofore inaccessible 3-aroyl- and 3-acyl-1,2,4-thiadiazoles 5 in 17-79% yields" @default.
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- W2026677369 date "2010-08-20" @default.
- W2026677369 modified "2023-09-23" @default.
- W2026677369 title "ChemInform Abstract: Reactions of Tetrasulfur Tetranitride with Bromomethyl Ketones. One- Pot Synthesis of 3,5-Diaroyl- and 3,5-Diacyl-1,2,4-thiadiazoles." @default.
- W2026677369 cites W2953304886 @default.
- W2026677369 doi "https://doi.org/10.1002/chin.199317172" @default.
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