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• W2026775240 abstract "Two new three-dimensional fluoroindium phosphates, In4(PO4)4(H2O)4F2·C6H14N2 1 and In8(PO4)8(H2O)8F4·(C5H14N2)2 2, have been prepared under hydrothermal conditions by using triethylenediamine and 1-methylpiperazine as templates, respectively. They are characterized by inductively coupled plasma analysis, elemental analysis, fluoride ion-selective electrode, IR spectra and thermogravimetric analysis. The structures have been solved by single-crystal X-ray diffraction. Both the compounds crystallize in the monoclinic system, space group P21/n (No.14). Crystal data for 1, M=1063.42, a=10.3161(4)Å, b=12.7490(3)Å, c=17.9127(6)Å, β=102.476(2)°, V=2300.25(13)Å3, Z=4. Crystal data for 2, M=2102.80, a=18.4673(6)Å, b=12.7117(5)Å, c=20.4705(7)Å, β=108.566(2)°, V=4555.4(3)Å3, Z=4. They exhibit the same topological structure and are built up from vertex linking InO4(H2O)2, InO4FH2O and InO4F2 octahedral and PO4 tetrahedral units, forming 6-membered ring channels along the a direction and two types of 8-membered ring channels along the b direction. The diprontonated triethylenediamine and 1-methylpiperazine molecules are entrapped in 8-membered ring channels." @default.
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• W2026775240 date "2004-11-01" @default.
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• W2026775240 title "Hydrothermal synthesis and characterization of two new three-dimensional fluoroindium phosphates In4(PO4)4(H2O)4F2·C6H14N2 and In8(PO4)8(H2O)8F4·(C5H14N2)2" @default.
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• W2026775240 doi "https://doi.org/10.1016/j.jssc.2004.06.049" @default.
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