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- W2026931433 abstract "Abstract Summary: ATRP of butyl α ‐fluoroacrylate (FABu) was carried out at 90 °C using methyl 2‐bromoisobutyrate (2‐MBiB) as initiator and the homogeneous catalyst CuBr/1,1,4,7,10,10‐hexamethyltriethylenetetramine (HMTETA). Telechelic oligomers were obtained by coupling the bromo terminated polymers in the presence of Cu (0) and 2,2′‐bipyridyl ligand. The 1 H and 19 F NMR, SEC and MALDI TOF analyses show that the poly(FABu) chains recombination was the main reaction (80% yield). About 20% of disproportionation reaction also occurs in the process, whereas transfer reactions can be neglected. Compounds produced by recombination, disproportionation and transfer during the coupling reaction of poly(FABu) oligomers. magnified image Compounds produced by recombination, disproportionation and transfer during the coupling reaction of poly(FABu) oligomers." @default.
- W2026931433 created "2016-06-24" @default.
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- W2026931433 date "2004-09-20" @default.
- W2026931433 modified "2023-10-11" @default.
- W2026931433 title "Synthesis of Telechelic Oligomers via Atom Transfer Radical Polymerization, 3" @default.
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- W2026931433 doi "https://doi.org/10.1002/macp.200400187" @default.
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