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- W2027435107 abstract "Abstract Reaction of Ni(acetate) 2 · 6H 2 OO with a potentially heptentate Schiff base ligand, tris[4-(2-thienyl)-3-aza-3-butenyl]amine [(thiophene) 3 ttren], resulted in the formation of an unexpected octahedral Ni I c complex with an NiN 4 core and the remaining two coordination sites occupied by solvent molecules. An X-ray crystal structure of the complex established the unusual cleavage at one of the three α-imino bonds and revealed that it deviates from the usual mono-capped trigonal prismatic coordination polyhedron designed for this type of complex. The complex molecule has an approximate plane of symmetry ( Cs ) r) rather than the three-fold axis ( C 3 )) normally observed for this type of complex and is the first example where the apical ‘unique’ nitrogen approaches the Ni I a as closely as the other three nitrogens of the ligand." @default.
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- W2027435107 date "1995-02-01" @default.
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- W2027435107 title "Unusual coordination of tripodal NN3SS3 donor ligand with nickel(II): Single crystal X-ray structure of [Ni{H2NCH2CH2N(CH2CH2NCH (C4H3S))2} (CH3CN)(H2O)](PF6)2" @default.
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- W2027435107 doi "https://doi.org/10.1016/0277-5387(94)00274-i" @default.
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