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- W2027465002 abstract "As a part of an investigation on the effect of water vapor on the thermal behavior of cyclo-phosphates, Mn3H2(P4O12)2·9.5H2O Mn3H2(P4m)2·9.5H2O was examined by means of DTA-TG, X-ray analysis, and HPLC-FIA. Mn3H2(P4m)2·9.5H2O lost the water of crystallization at about 145 °C. In a temperature range 165–265 °C, Mn3H2(P4m)2 anhydride decomposed to form oligophosphates(Poligo). At temperatures below 200 °C, the amounts of Poligo were more abundant under humid conditions than under dry conditions. At 265–450 °C, Poligo changed partially into polyphosphates (Ppoly) and insoluble highpolyphosphates(Phigh poly). The dehydration and condensation reactions proceeded faster under dry conditions than under humid conditions, where gradual water evolution was noted over the temperature range of 265 to 450 °C. The stable crystalline Phigh poly, Mn(PO3)2, was produced at temperatures above 450 °C, where the product was not affected by the water vapor." @default.
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- W2027465002 date "1992-03-01" @default.
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- W2027465002 title "Effect of Water Vapor on the Thermal Behavior of Manganesecyclo-Tetraphosphate" @default.
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- W2027465002 doi "https://doi.org/10.1246/bcsj.65.777" @default.
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