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- W2027503580 abstract "Synthetic routes to the title compounds were explored. 1,2,5,6-Tetraacetylperhydro-1,2,5,6-tetrazocine (6, 36%) was produced from ethylene glycol bis-p-toluenesulfonate and the potassium salt of 1,2-bis(N,N′ -diacetylhydrazino)ethane in refluxing mesitylene. Its acid-catalyzed hydrolysis led to perhydro-1,2,5,6-tetrazocine (9), an air-sensitive, crystalline solid, the first reported unsubstituted tetraazacyclooctane and the first example of an unsubstituted macrocycle incorporating two or more endocyclic hydrazino groups. 1,2-Bis(hydrazino)ethane (4) and diisobutyl oxalate in refluxing dimethylformamide gave 1,4-diamino-2,3-diketopiperazine (11) rather than 3,4-diketoperhydro-1,2,5,6-tetrazoeine (12). The acid-catalyzed reaction of benzil with 4 gave 3,4,7,8-tetraaza-1,2,9,10-tetraphenyl-2,8-dccadien-1,10-dione (20)." @default.
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- W2027503580 date "1976-02-01" @default.
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- W2027503580 title "Synthesis of perhydro-1,2,5,6-tetrazocine and derivatives" @default.
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- W2027503580 doi "https://doi.org/10.1002/jhet.5570130119" @default.
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