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• W2027607969 abstract "Abstract Complexes [Cp* 2 Mo 2 O 5 ] (Cp* = η 5 ‐C 5 Me 5 ) and [Cp* 2 Mo 2 O 4 ] were investigated by combined on‐line electrochemical (EC) reduction and electrospray‐ionization mass spectrometry (ESI‐MS) techniques in a trifluoroacetic acid buffered water/methanol solution. The reduction products at the larger negative potentials are identical for both compounds. The studies reveal the existence of a wide range of previously unknown di‐ and trinuclear Mo V , Mo IV , Mo III , and mixed‐valence complexes that were identified on the basis of their masses and characteristic isotope patterns. The structures of the initial compounds and the product of electroreduction with m / z = 713−729 were supported by in situ MS n experiments that allowed the elucidation of the fragmentation pathway for the collision‐induced dissociation. (© Wiley‐VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, Germany, 2003)" @default.
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• W2027607969 date "2003-06-01" @default.
• W2027607969 modified "2023-10-16" @default.
• W2027607969 title "Reduction of [(C ₅ Me ₅ ) ₂ Mo ₂ O ₅ ] and [(C ₅ Me ₅ ) ₂ Mo ₂ O ₄ ] in Methanol/Water/Trifluoroacetate Solutions Investigated by Combined On‐Line Electrochemistry/Electrospray‐Ionization Mass Spectrometry" @default.
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• W2027607969 doi "https://doi.org/10.1002/ejic.200200627" @default.
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