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- W2027688936 abstract "The reaction of MH4 (M = Si, Ge) with Fe2(CO)9 in hexane gives Si[Fe2(CO)8]2 or Ge[Fe2(CO)8]2 in 61 or 43% yield, respectively. A reproducible synthesis of Sn[Fe2(CO)8]2 from “[Fe2(CO)8]2− and SnCl4 in thf is also described. The X-ray crystal structure of Si[Fe2(CO)8]2 shows two mutually perpendicular SiFe2 triangles linked at the common spiro-silicon atom, with each iron atom carrying four terminal CO ligands. Average bond lengths are: FeSi 2.345(4), FeFe 2.795(3) Å." @default.
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- W2027688936 date "1988-08-01" @default.
- W2027688936 modified "2023-10-16" @default.
- W2027688936 title "Improved syntheses of M[Fe2(CO)8]2 (M = Si, Ge or Sn) and the X-ray crystal structure of Si[Fe2(CO)8]2" @default.
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- W2027688936 doi "https://doi.org/10.1016/0022-328x(88)80376-0" @default.
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