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- W2027755016 abstract "Silicon microreactors have been coated with mixed-metal Fe−Co Fischer−Tropsch catalysts in alumina sol−gel for conversion of syngas (CO + H2) to higher alkanes. Characterization of the nanocatalysts using scanning electron microscopy, energy-dispersive X-ray, atomic force microscopy, and Brunauer−Emmett−Teller surface area measurements, packaging, and the reaction results from a mass spectrometer at controlled temperatures (200−260 °C) and pressure (1 atm) with varying H2:CO ratios from 1:1 to 10:1 are described. The catalyst does not adequately infiltrate the 5-μm channels; it coats nicely the 25-μm channels. The initial results are consistent with a lower conversion of CO (∼32%) in a 5-μm-channel reactor and a higher conversion (∼52%) in a 25-μm-channel reactor. The selectivity to propane (∼80%) is not affected by the width of the microchannels. The activity of the sol−gel-encapsulated catalyst before and after the reactions is estimated from its magnetic properties using a vibrating sample magnetometer." @default.
- W2027755016 created "2016-06-24" @default.
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- W2027755016 date "2005-06-23" @default.
- W2027755016 modified "2023-10-12" @default.
- W2027755016 title "Microreactors for Syngas Conversion to Higher Alkanes: Characterization of Sol−Gel-Encapsulated Nanoscale Fe−Co Catalysts in the Microchannels" @default.
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- W2027755016 doi "https://doi.org/10.1021/ie0487484" @default.
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