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• W2028087946 abstract "Abstract A range of potential boron‐based ligand precursors has been synthesized starting from [{Br 2 B( η 5 ‐C 5 H 4 )}Mn(CO) 3 ] ( 1 ) via salt elimination reactions. These comprise ligand precursors suitable for the preparation of i) ansa ‐metallocenes such as [CymB( η 1 ‐C 5 H 5 ) 2 ] ( 2 ), [CymB(1‐C 9 H 7 ) 2 ] ( 3a ), and [CymB(3‐C 9 H 7 ) 2 ] ( 3b ), ii) constrained geometry complexes such as [CymB(Br)N(H) t Bu] ( 5 ) as well as iii) ansa ‐diamido complexes such as [CymB{N(H)Ph} 2 ] ( 4 ) and [CymB{N(H) t Bu} 2 ] ( 6 ) (Cym = cymantrenyl, C 5 H 5 = cyclopentadienyl, C 9 H 7 = indenyl). Furthermore, we present the hydrolysis of 1 , leading to the three‐fold cymantrenyl‐substituted boroxine [{OB( η 5 ‐C 5 H 4 )}Mn(CO) 3 ] 3 ( 7 ). All new compounds have been characterized by multinuclear NMR spectroscopic techniques and in the case of 1 and 7 by X‐ray diffraction analyses." @default.
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• W2028087946 date "2007-10-01" @default.
• W2028087946 modified "2023-10-12" @default.
• W2028087946 title "[{Br₂B(<i>η</i>⁵‐C₅H₄)}Mn(CO)₃] – A versatile Precursor for Boron‐based Ligands" @default.
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• W2028087946 doi "https://doi.org/10.1002/zaac.200700207" @default.
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