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- W2028126263 abstract "Cs3V2O4F5 and phases in the systems Cs3Mo2O6F3-Cs3V2O2F7 and Cs3Mo2O6F3-Cs3V2O4F5 crystallize in the hexagonal space group P63/mmc with a Cs3Fe2F9-type structure and thus contain face-shared bioctahedral M2(O,F)9 units. The structures of Cs3V2O4F5(a = 6.319(1) Å, c = 14.850(2) Å) and CS3V1.5Mo0.5O3F6(a = 6.359(2) Å, c = 14.999(4) Å) were determined on single crystals. In Cs3V2O4F5, which exhibits a substructure with a' = a and c' = c3, the vanadium atoms are statistically disordered over all (O,F)6 octahedral holes. Vibrational spectra show that oxygen occupies exclusively terminal positions in the individual [V2O4F5]3− anions. In Cs3V1.5Mo0.5O3F6 the M2(O,F)9 bioctahedra with M Mo and/or V are strictly ordered. Raman bands show the presence of VO (terminal), MoO2 (terminal) and oxygen bridge bonds. In Cs3VMoO5F4(a = 6.338(2) Å, c = 14.920(3) Å) the binuclear species [O2FVOF2MoO2F]3− is predominant." @default.
- W2028126263 created "2016-06-24" @default.
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- W2028126263 date "1982-10-01" @default.
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- W2028126263 title "Structural and spectroscopic studies of Cs3V2O4F5 and of isostructural phases in the Cs3Mo2O6F3-Cs3V2O2F7 and Cs3Mo2O6F3-Cs3V2O4F5 Systems" @default.
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- W2028126263 doi "https://doi.org/10.1016/0022-5088(82)90091-1" @default.
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