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- W2028130536 abstract "Abstract The reaction of 1-hydroxybenzotriazole, btaOH, with nickel(II) acetate tetrahydrate, in the absence of an external base, has been investigated. The reaction of Ni(O2CMe)2 · 4H2O with one equivalent of btaOH in nPrOH leads to the the first structurally characterized tridecanuclear nickel(II) cluster and the biggest metal/btaOH or btaO− cluster discovered to date, [Ni13(OH)6(O2CMe)8(btaO)12(H2O)6(nPrOH)4] · 6.6H2O · 4(nPrOH) (1 · 6.6H2O · 4(nPrOH)). The centrosymmetric molecule contains the {Ni13(μ3-ΟΗ)6(μ3-ONNNR)12}8+ core (R– = C6H4–) and is characterized by competitive antiferromagnetic exchange interactions within its pentanuclear subunits containing the μ3-ΟΗ− bridges. The reaction of 1 with an excess of N 3 - ions in refluxing MeOH has led to the azido-bridged product [Ni13(N3)6(O2CMe)8(btaO)12(MeOH)10] (2), in which the spin frustration observed in 1 seems to disappear." @default.
- W2028130536 created "2016-06-24" @default.
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- W2028130536 date "2009-06-01" @default.
- W2028130536 modified "2023-10-03" @default.
- W2028130536 title "High-nuclearity nickel(II) clusters: Ni13 complexes from the use of 1-hydroxybenzotriazole" @default.
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- W2028130536 doi "https://doi.org/10.1016/j.poly.2008.10.036" @default.
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