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- W2028168045 abstract "From the temperature dependence of the rotational frequency of a nitroxide spin probe dispersed in poly(vinyl acetate) the size of the polymer segment involved in the glass to rubber relaxation can be estimated. The calculation is based on a free volume model which relates f, the ratio of the volumes of the spin probe and the polymer segment, to the rotational frequency of the probe. An increase in f with increasing size of the probe is demonstrated. Saturation transfer electron spin resonance spectra of two nitroxide probes are shown to undergo a rapid change with temperature at a temperature TR which is characteristic of both the probe and its environment. TR corresponds to a pseudo-isofrequency point and is analogous to, though at a lower characteristic frequency than, the widely-used parameter T50G. For the systems examined, TR correlates with the glass to rubber relaxation." @default.
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- W2028168045 date "1986-02-01" @default.
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- W2028168045 title "E.s.r. and saturation transfer e.s.r. spectroscopy of spin-probed poly(vinyl acetate): A new spectral transition correlating with glass transition temperature" @default.
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- W2028168045 doi "https://doi.org/10.1016/0032-3861(86)90325-3" @default.
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