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- W2028236437 abstract "The preparation and ESR-spectroscopic characterization of radical complexes with L = 4,4′-bipyridine is described, where MRn = BePh, MgPh, ZnPh, −BEt3, GaMe2, InMe2 and SiMe3. While the bis(trimethylsilyl) derivative could be obtained via one-electron oxidation of the corresponding 4,4′-(1H, 1′H)-bi-pyridinylidene, the other complexes were prepared by the reaction of 4,4′-bipyridine with potassium and the organometal MRn+1 or the halide XMRn in THF. Use of organo-cadmium or -thallium compounds in such a procedure leads to deposition of the metals. The Grignard reagents MgPh2 and BrMgPh reduce 4,4′-bipyridine in an electron transfer process to yield an unsymmetrical complex. The new organometallic 4,4′-bipyridinium (“violence”) radical complexes can be incorporated into a series of related radicals which exhibits the sensitivity of the unpaired electron distribution towards metal coordination." @default.
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- W2028236437 date "1983-01-01" @default.
- W2028236437 modified "2023-10-05" @default.
- W2028236437 title "Metallaviolenes. An ESR study" @default.
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- W2028236437 doi "https://doi.org/10.1016/s0022-328x(00)98503-6" @default.
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