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• W2028341583 startingPage "G83" @default.
• W2028341583 abstract "The electrochemical polymerization of azure B in aqueous sulfuric acid solution has been carried out by use of cyclic voltammetry. A dark blue film, i.e., poly(azure B), was deposited on the glassy carbon electrode (GCE) and exhibited good electrochemical reversibility and fast-charge transfer ability in 0.5 M Na2SO4 of pH 3.0. The pH dependence of poly(azure B) polymerized on the GCE is different from that polymerized on platinum foil. The anodic and cathodic peak currents of poly(azure B) are proportional to the square root of scan rate between 25 and 600 mV s−1, indicating the electrode reaction process of the polymer is diffusion-controlled. Visible and FT-IR spectra of poly(azure B) were also acquired, which are different from those of the monomer. Scanning electron microscopy shows that the poly(azure B) film contains irregular nano-pores, and this makes it a potential material for the construction of biosensors. Cyclic voltammograms of poly(azure B) were determined at different temperatures, and the peak currents increase with increasing temperature. From the temperature dependence of the redox currents, the activation energies of the anode and cathode reactions of poly(azure B) were calculated to be 11.1 and 9.2 kJ mol−1, respectively." @default.
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• W2028341583 date "2013-01-01" @default.
• W2028341583 modified "2023-09-26" @default.
• W2028341583 title "Electrochemical Synthesis and Properties of Poly(azure B)" @default.
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• W2028341583 doi "https://doi.org/10.1149/2.071306jes" @default.
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