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- W2028367803 abstract "Abstract On‐line solid phase extraction (SPE) coupled with reversed phase high performance liquid chromatography (PRHPLC‐DAD) detection was developed for the determination of tetrachloroethene (PCE), trichloroethylene (TCE), and the metabolites [cis‐1,2‐dichloroethene (cis‐DCE), trans‐1,2‐dichloroethene (trans‐DCE)] in ground waters. The PCE, TCE, and their metabolites were directly concentrated and cleaned‐up on the cartridge, and separated by a C18 column with UV at 210 nm. Five sorbents (C8, C18, PLRP‐S, PRP‐1, and Bond‐Elut Env) were evaluated to concentrate these compounds. The recoveries of the compounds were significantly improved by the addition of 10% (v/v) acetonitrile (ACN) to the sample before loading. When a 50 mL sample spiked with 1 µg/L was loaded onto PLRP‐S sorbent, the recoveries of the compounds ranged from 66.7% to 104.5%. The determination of these compounds was possible with detection limits less than 0.05 µg/L. The method was compared with a gas chromatography (GC) for the determin..." @default.
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- W2028367803 date "2004-01-01" @default.
- W2028367803 modified "2023-09-27" @default.
- W2028367803 title "Determination of Tetrachloroethene, Trichloroethylene, and Their Metabolites at Trace Levels in Ground Waters by On‐Line Solid Phase Extraction/HPLC" @default.
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