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- W2028421954 abstract "Asymmetric iodolactonization of γ- and δ-unsaturated carboxylic acids has been explored in the presence of six different chiral organocatalysts 5-8. The catalyst 6b was found to facilitate the cyclization of 5-arylhex-5-enoic acids 1 to the corresponding iodolactones 2 with up to 96% ee. By this protocol, unsaturated carboxylic acids are converted enantioselectively to synthetically useful δ-lactones in high yields using commercially available NIS. Apparently, both hydrogen bonding and aryl/aryl interactions are important for efficient stereodifferentiation." @default.
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- W2028421954 date "2012-11-13" @default.
- W2028421954 modified "2023-10-17" @default.
- W2028421954 title "Asymmetric Iodolactonization Utilizing Chiral Squaramides" @default.
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- W2028421954 doi "https://doi.org/10.1021/ol302798g" @default.
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