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- W2028432859 abstract "The structures of [RhCl(CO) (1)] and [PdCl2 (1)], where 1 is the bidentate ligand (C6H5)2P·CH2·C18H10· CH2·P(C6H5)2, have been determined from threedimensional X-ray counter data collected on single crystals of the C6H5·CN solvates. The two compounds are isomorphous and crystallize in the triclinic system, space group P 1, Z = 2: a = 14.580 (8), b = 13.029 (10), c = 11.909 (6) Å, α = 106.33 (5), β = 100.47 (4), γ = 95.73 (5)° for the rhodium complex; a = 14.361 (5), b = 13.044 (7), c = 11.897 (4) Å, α = 105.97 (4), β = 100.27 (3), γ = 94.76 (4)°, for the palladium complex. In both complexes the metal atom is four-coordinate with slightly distorted square-planar configuration. In both cases the ligand 1 spans trans positions with M-P bond lengths in the ranges of the literature data. Also the other bond distances fall in regular ranges. Ligand 1 has almost the same conformation in both complexes and is characterized by a strong out-of-plane deformation of the benzophenanthrene system as a consequence of severe overcrowding." @default.
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- W2028432859 title "Transition-metal complexes with bidentate ligands spanningtrans-positions. V. Crystal and molecular structures of complexes [RhCl(CO) (1)] and [PdCl2(1)]; 1 = 2,11-bis (diphenylphosphinomethyl)benzo [c]phenanthrene" @default.
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