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- W2028590963 abstract "Capillary electrophoresis with amperometric detection is evaluated for the simultaneous determination of 2-aminothiazole (A), 2-aminobenzothiazole (AB), 2-mercaptobenzothiazole (AM). The cyclic voltammogram, hydrodynamic voltammogram, effect of pH, concentration of buffer and separation voltage on the separation and the detection were studied. The conditions were optimized as follows: 50 mM phosphate buffer, pH 6.0, 2s at 17.5 kV sample injection, separation at 17.5 kV, 1.2 V as detection potential. The method provided low detection limit as 0.5 µM, 0.05 µM and 0.01 µM, wide linear range 2–200 µM, 10–200 µM and 0.025–100 µM for A, AB, and AM, respectively. The variations in peak current and migration time for 15 consecutive injections of a standard containing 5 µM each compound were 3.7, 2.1, and 3.9 %, and 1.2, 0.8, and 1.2 %, for A, AB and AM, respectively. This method was employed to analyze river water." @default.
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- W2028590963 date "2000-07-01" @default.
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- W2028590963 title "Simultaneous Determination of 2-Aminothiazole, 2-Aminobenzothiazole and 2-Mercaptobenzothiazole by Capillary Electrophoresis with End-Column Amperometric Detection" @default.
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- W2028590963 doi "https://doi.org/10.1002/1521-4109(200007)12:11<821::aid-elan821>3.0.co;2-4" @default.
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