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- W2028598846 abstract "New rare earth bismuth oxynitrates,RBi2O4NO3(R: Y, Sm, Eu, Gd, Tb, Dy, Er, Yb) were prepared with low temperature hydrothermal reactions using NaBiO3·nH2O andR(NO3)·nH2O as starting materials. These rare earth bismuth oxynitrates crystallized in the tetragonal system with space groupP4mmandZ=1. The lattice parameters depend on the ionic radius of rare earth atoms and range froma=3.8470(1) andc=10.1762(7) Å forR=Yb toa=3.9038(1) andc=10.2370(5) Å forR=Sm. The crystal structure forR=Y was refined using neutron powder diffraction data, with the finalRfactors beingRWP=4.35,RP=3.29,RI=5.39, andRF=4.40%.RBi2O4NO3is isostructural withR′xBi3−xO4X(R′: La, Ce, Nd, Eu, Gd;X: Cl, Br, Se) having a layered structure based on (RBi2O4)+and (NO3)−layers. There are three kinds of metal atom positions, all coordinated by eight oxygens; one is occupied by Y atoms and the other two are filled with Bi atoms. On heating above 500°C this compound decomposes to the solid solution (R,Bi)2O3accompanied by the evolution of NO and O2." @default.
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- W2028598846 date "1998-09-01" @default.
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- W2028598846 title "Preparation and Crystal Structure of New Rare Earth Bismuth Oxynitrates:RBi2O4NO3(R: Y, Sm, Eu, Gd, Tb, Dy, Er, Yb)" @default.
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- W2028598846 doi "https://doi.org/10.1006/jssc.1998.7849" @default.
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