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- W2028876886 abstract "Successful use of LC–NMR and LC–MS for rapid identification of an impurity in a novel antifungal drug icofungipen has been demonstrated. Complementary information obtained from the two methods made it possible to determine the structure of A1 prior to its isolation and purification. Stop-flow LC–NMR (1H and DQFCOSY), LC–MS and LC–MS/MS spectra have shown that A1 is structurally related to icofungipen. It was later isolated and prepared synthetically and its structure was corroborated by high-resolution NMR spectroscopy." @default.
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- W2028876886 date "2009-08-01" @default.
- W2028876886 modified "2023-09-23" @default.
- W2028876886 title "LC–NMR and LC–MS identification of an impurity in a novel antifungal drug icofungipen" @default.
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- W2028876886 doi "https://doi.org/10.1016/j.jpba.2009.03.017" @default.
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