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- W2028933086 abstract "In situ synchrotron X-ray powder diffraction was used to study the crystallization of microporous aluminophosphate and of Mg2+-, Mn2+-, Co2+-, and Zn2+-substituted aluminophosphates. The gels contained the templates 2-(diethylamino)ethanol, di-n-propylamine, triethylamine, and tripropylamine and were heated in quartz glass capillaries at temperatures up to 200 °C. The main crystalline reaction products formed were AlPO4 (tridymite type), APO-5 (AFI), APO-11 (AEL), MgAPO-5 (AFI), MnAPO-5 (AFI), CoAPO-5 (AFI), ZnAPO-39 (ATN), and ZnAPO-47 (CHA). A kinetic analysis of the crystallization of MnAPO-5 (AFI) and ZnAPO-47 (CHA) was performed using isothermal in situ synchrotron X-ray powder diffraction data. The apparent activation energies for the hydrothermal nucleation of MnAPO-5 (AFI) and ZnAPO-47 (CHA) were 161(6) and 112(3) kJ/mol, respectively. The crystallization of MnAPO-5 could be modeled using a first-order expression giving an apparent activation energy of the crystal growth of 81(6) kJ/mol. The crystallization of ZnAPO-47 was more complex, and the crystallization curves could not be described using simple kinetic expressions." @default.
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- W2028933086 date "1998-04-29" @default.
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- W2028933086 title "In Situ Synchrotron X-ray Powder Diffraction Studies of Crystallization of Microporous Aluminophosphates and Me<sup>2+</sup>-Substituted Aluminophosphates" @default.
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- W2028933086 doi "https://doi.org/10.1021/cm980049s" @default.
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