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W202894664 endingPage "334" @default.
W202894664 startingPage "291" @default.
W202894664 abstract "This chapter provides a summary of the recently published solid-phase microextraction (SPME) studies and reviews in the field of food and fragrance analysis, together with several case studies highlighting the advantages and disadvantages of this technique compared to other commonly used isolation techniques. Food is a very complex matrix, and several procedures are typically used in order to prepare a food sample for the final gas chromatography (GC), liquid chromatography (LC), or other analysis. In order to prepare a representative sample, solid matrices need to be homogenized and liquid or gaseous samples must be properly stirred prior to the isolation of the target analytes from the examined matrix. Solid-phase microextraction has become one of the most generally used extraction procedures. When it comes to SPME method development for food/fragrance samples, optimization of the extraction process must be made considering the complexity of examined samples as well as the fact that trace target analytes may be co-extracted with interfering matrix components. The parameters that are typically critically evaluated involve the implementation of selective extraction phases towards a specific group of target analytes that simultaneously demonstrate substantially reduced selectivity and sensitivity for interfering non-targeted matrix components. In those cases involving non-targeted fingerprinting and profiling food applications, the objective of coating selection is the opposite: comprehensive metabolite coverage requiring a non-selective extraction phase. These critical requirements have been recently addressed in order to standardize SPME coating selection for a wide range of analytes frequently encountered in food/fragrance matrices and having differing physico-chemical properties and evaluate the performance of commercial coatings in non-targeted studies of food/plant systems (metabolomics)." @default.
W202894664 created "2016-06-24" @default.
W202894664 creator A5080374957 @default.
W202894664 creator A5080934776 @default.
W202894664 date "2012-01-01" @default.
W202894664 modified "2023-09-25" @default.
W202894664 title "Application of Solid-Phase Microextraction in Food and Fragrance Analysis" @default.
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