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- W2029016150 abstract "The thermal decomposition and mass spectra of the N-phenyl- (1), N,N′-diphenyl- (2), and N,N′,N′-triphenylphosphoric triamides (3) were investigated. DTA-TG/DTG, TG-TRAP-GC/MS measurements, IR spectroscopic analyses, mass spectrometric analyses, HPLC analyses, and a kinetic study were carried out to investigate the thermal decomposition. From the analytical results, it was suggested that 1 decomposed while liberating ammonia and aniline, and condensed in several stages; its thermal products at about 160 °C contained 2. Compound 2 decomposed and condensed to form some condensed products at about 200 °C; its thermal products also contained 3. Compound 3 decomposed while liberating aniline to form a cyclic dimer, while the existence of other thermal products was also observed; the cyclic dimer further pyrolyzed in several stages, and 1 and 2 formed a similar condensed product in the 400 to 500 °C temperature range, though that for 3 was different. In addition, the apparent activation energy of the thermal de..." @default.
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- W2029016150 date "1996-02-01" @default.
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- W2029016150 title "Thermal Decomposition and Mass Spectra of the<i>N</i>-Phenyl-,<i>N</i>,<i>N</i>′-Diphenyl-, and<i>N</i>,<i>N</i>′,<i>N</i>″-Triphenylphosphoric Triamides" @default.
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- W2029016150 doi "https://doi.org/10.1246/bcsj.69.367" @default.
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